HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Acetone → 4-(Bromomethyl)-2,2-dimethyl-1,3-dioxolane
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Acetone | HCID 180 | — |
| Edukt | 3-Bromo-1,2-propanediol | HCID 20827 | — |
| Edukt | Sulfuric acid magnesium salt (1:1) | HCID 24083 | — |
| Produkt | 4-(Bromomethyl)-2,2-dimethyl-1,3-dioxolane | HCID 169759 | — |
Reaktionsschritte
An acetone solution of bromomethyl ethylene glycol is refluxed for 24 hours in the presence of anhydrous magnesium sulfate. The cooled reaction mixture is filtered and the solvent is removed to provide a residual crude product.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04762912 |
| Quelldatensatz | uspto-grants-1988_08 |
| ORD ID | ord-01f407b26c404daab6db59143a8e4364 |
| Quellennotiz | uspto-grants-1988_08 |