HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3-Methoxybenzenethiol → 3-(4-Bromo-phenyl)-2-methyl-benzo[b]thiophen-6-ol
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3-Methoxybenzenethiol | HCID 84989 | — |
| Edukt | 2,4'-Dibromopropiophenone | HCID 603907 | — |
| Produkt | 3-(4-Bromo-phenyl)-2-methyl-benzo[b]thiophen-6-ol | HCID 22313887 | — |
Reaktionsschritte
In analogy to examples 26.1–26.3, 3-mercaptoanisole and 2,4′-dibromopropiophenone were converted to yield 3-(4-bromo-phenyl)-2-methyl-benzo[b]thiophen-6-ol as colorless amorphous solid, MS: 318 (M, 1Br).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07173043B2 |
| Quelldatensatz | uspto-grants-2007_02 |
| ORD ID | ord-bb9043df9e7a4ceb98eb945800e02e50 |
| Quellennotiz | uspto-grants-2007_02 |