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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 35000Erstellt: 23. Oktober 2026

Oxalic acid dihydrate → N-(1-phenyl-3-pyrrolidinopropyl)quinaldinamide oxalate

https://huagongshe.com/de/reaction/35000

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktOxalic acid dihydrateHCID 61373—
EduktN-(1-phenyl-3-pyrrolidinopropyl)quinaldinamideHCID 67930046—
LösungsmittelEthanolHCID 702—
ProduktN-(1-phenyl-3-pyrrolidinopropyl)quinaldinamide oxalateHCID 6793006596%

Reaktionsschritte

In ethanol were dissolved 259 mg (0.72 mmol.) of N-(1-phenyl-3-pyrrolidinopropyl)quinaldinamide and 91 mg of oxalic acid dihydrate. The resulting solution was evaporated under reduced pressure to remove the solvent. The residue was recrystallized from a mixture of acetone (6 ml) and diethyl ether (3 ml) to obtain 310 mg (yield: 96%) of the subject compound as a white crystalline product.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04764617
Quelldatensatzuspto-grants-1988_08
ORD IDord-2aec0cad6b69427e995ed42842590707
Quellennotizuspto-grants-1988_08