HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Oxalic acid dihydrate → N-(1-phenyl-3-pyrrolidinopropyl)quinaldinamide oxalate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Oxalic acid dihydrate | HCID 61373 | — |
| Edukt | N-(1-phenyl-3-pyrrolidinopropyl)quinaldinamide | HCID 67930046 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | N-(1-phenyl-3-pyrrolidinopropyl)quinaldinamide oxalate | HCID 67930065 | 96% |
Reaktionsschritte
In ethanol were dissolved 259 mg (0.72 mmol.) of N-(1-phenyl-3-pyrrolidinopropyl)quinaldinamide and 91 mg of oxalic acid dihydrate. The resulting solution was evaporated under reduced pressure to remove the solvent. The residue was recrystallized from a mixture of acetone (6 ml) and diethyl ether (3 ml) to obtain 310 mg (yield: 96%) of the subject compound as a white crystalline product.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04764617 |
| Quelldatensatz | uspto-grants-1988_08 |
| ORD ID | ord-2aec0cad6b69427e995ed42842590707 |
| Quellennotiz | uspto-grants-1988_08 |