Fumaric Acid → N-[1-(2-methylphenyl)-3-piperidinopropyl]quinaldinamide fumarate
Reaktionsgleichung
[CH3:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[CH:8]([NH:17][C:18]([CH2:20][C:21]1[CH:30]=[CH:29][C:28]2[C:23](=[CH:24][CH:25]=[CH:26][CH:27]=2)[N:22]=1)=[O:19])[CH2:9][CH2:10][N:11]1[CH2:16][CH2:15][CH2:14][CH2:13][CH2:12]1.[C:31]([OH:38])(=[O:37])/[CH:32]=[CH:33]/[C:34]([OH:36])=[O:35]>>[C:31]([OH:38])(=[O:37])/[CH:32]=[CH:33]/[C:34]([OH:36])=[O:35].[CH3:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[CH:8]([NH:17][C:18]([CH2:20][C:21]1[CH:30]=[CH:29][C:28]2[C:23](=[CH:24][CH:25]=[CH:26][CH:27]=2)[N:22]=1)=[O:19])[CH2:9][CH2:10][N:11]1[CH2:12][CH2:13][CH2:14][CH2:15][CH2:16]1Komponenten
3
Versuchsvorschrift
The procedure of Example 11 was repeated using 736 mg (1.9 mmol.) of N-[1-(2-methylphenyl)-3-piperidinopropyl]quinaldinamide and 220 mg (1.9 mmol.) of fumaric acid, to obtain 708 mg (yield: 74%) of the subject compound.
Quellen und Nachweise
- ORD-Eintrag
- ord-e0a55bbd18f149efb6cadcc27278e15e
- Quelldatensatz
- uspto-grants-1988_08