HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Oxalic acid dihydrate → N-[1-(4-methoxyphenyl)-3-piperidinopropyl]quinaldinamide oxalate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Oxalic acid dihydrate | HCID 61373 | — |
| Edukt | N-[1-(4-methoxyphenyl)-3-piperidinopropyl]quinaldinamide | HCID 67930051 | — |
| Produkt | N-[1-(4-methoxyphenyl)-3-piperidinopropyl]quinaldinamide oxalate | HCID 67930076 | 70% |
Reaktionsschritte
The procedure of Example 7 was repeated using 1.03 g (2.56 mmol.) of N-[1-(4-methoxyphenyl)-3-piperidinopropyl]quinaldinamide and 323 mg (2.56 mmol.) of oxalic acid dihydrate, to obtain 884 mg (yield: 70%) of the subject compound as a white powdery product upon recrystallization from 8 ml of ethanol.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04764617 |
| Quelldatensatz | uspto-grants-1988_08 |
| ORD ID | ord-5116b757d2fc4b29bf10d174261fb24e |
| Quellennotiz | uspto-grants-1988_08 |