HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Sodium ethoxide → ethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6carboximidate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Sodium ethoxide | HCID 2723922 | — |
| Edukt | 5,7-dihydro-6H-dibenz[c,e]azepine-6carbonitrile | HCID 19833886 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | ethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6carboximidate | HCID 19833914 | — |
Reaktionsschritte
starting from 5,7-dihydro-6H-dibenz[c,e]azepine-6-carbonitrile and sodium ethylate in ethanol there is obtained ethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate and therefrom with hydrochloric acid in alcohol there is obtained the hydrochloride, m.p. 158° C. (with decomposition);
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04766115 |
| Quelldatensatz | uspto-grants-1988_08 |
| ORD ID | ord-ad64697779764f5296b06bd50992d95c |
| Quellennotiz | uspto-grants-1988_08 |