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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 35194Erstellt: 24. Oktober 2026

Sodium Carbonate → HCID 15612244, Verbindung

https://huagongshe.com/de/reaction/35194

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktSodium CarbonateHCID 10340—
Edukt2-(3-Pyridylmethyl)-6-(2-methyl-1,3-dioxolan-2-yl)naphthaleneHCID 15612243—
LösungsmittelHydrochloric AcidHCID 313—
ProduktHCID 15612244HCID 15612244101,3%

Reaktionsschritte

A solution of 150 mg of 2-(3-pyridylmethyl)-6-(2-methyl-1,3-dioxolan-2-yl)naphthalene in 15 ml of 1N hydrochloric acid was allowed to stand for 3 hours at room temperature. The solution was neutralized with sodium carbonate and extracted with methylene chloride. The organic layer was dried over sodium sulfate and the solvent removed under reduced pressure to give 130 mg of 2-(3-pyridylmethyl)-6-acetylnaphthalene as an oil.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04766127
Quelldatensatzuspto-grants-1988_08
ORD IDord-d087129627ad4ec4a8be14aecff590ba
Quellennotizuspto-grants-1988_08