2-Allylphenol → Benzoxazines
Reaktionsgleichung
[NH2:1][CH2:2][CH2:3][CH2:4][Si](OC)(OC)OC.[CH2:12]([C:15]1C=CC=C[C:16]=1[OH:21])[CH:13]=[CH2:14]>C1(C)C=CC=CC=1>[O:21]1[C:16]2[CH:15]=[CH:12][CH:13]=[CH:14][C:4]=2[CH:3]=[CH:2][NH:1]1Komponenten
4
Edukt 2
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Versuchsvorschrift
This compound was prepared according to the method described in the previous examples using 3-aminopropyltrimethoxysilane (17.9 g, 100 mmole), paraformaldehade (6.3 g, 210 mmole), 2-allyl-phenol (13.4 g, 0.1 mmole), and toluene (200 ml). The final product was obtained as a slightly yellow, mobile liquid. The yield was 94% of theory.
Aufarbeitung
- customThis compound was prepared
Quellen und Nachweise
- ORD-Eintrag
- ord-6358ad625d7f4fa781932705f29eec87
- Quelldatensatz
- uspto-grants-2004_06
- Patentnummer
- US06743852B2
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