HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Tert-butyl 4-benzylpiperazine-1-carboxylate → 1-Benzylpiperazine hydrochloride
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Tert-butyl 4-benzylpiperazine-1-carboxylate | HCID 584330 | — |
| Edukt | Ethanol hydrochloride | HCID 21887872 | — |
| Produkt | 1-Benzylpiperazine hydrochloride | HCID 2756653 | 97% |
Reaktionsschritte
To 1-benzyl-4-tert-butoxycarbonylpiperazine (3.12 g), saturated ethanol hydrochloride was added, followed by stirring for 90 minutes at room temperature. The solvent was distilled off under reduced pressure, followed by drying, whereby the title compound (2.73 g, 97%) was obtained as white powder.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06747023B1 |
| Quelldatensatz | uspto-grants-2004_06 |
| ORD ID | ord-33705c0319e7456583203d04feae1405 |
| Quellennotiz | uspto-grants-2004_06 |