tert-butyl 1H-pyrrole-2-carboxylate → 5,11-Dihydro-5,11-dimethyl-2-(2-pyrrolyl)-6H-dipyrido[3,2-b:2',3'-e][1,4]diazepin-6-one
Reaktionsgleichung
Cl[C:2]1[CH:3]=[CH:4][C:5]2[N:6]([CH3:19])[C:7](=[O:18])[C:8]3[CH:17]=[CH:16][CH:15]=[N:14][C:9]=3[N:10]([CH3:13])[C:11]=2[N:12]=1.C(OC([C:27]1[NH:28][CH:29]=[CH:30][CH:31]=1)=O)(C)(C)C>>[CH3:19][N:6]1[C:7](=[O:18])[C:8]2[CH:17]=[CH:16][CH:15]=[N:14][C:9]=2[N:10]([CH3:13])[C:11]2[N:12]=[C:2]([C:27]3[NH:28][CH:29]=[CH:30][CH:31]=3)[CH:3]=[CH:4][C:5]1=2Komponenten
3
Versuchsvorschrift
The title compound (mp 158°-160° C.) was prepared from 2-chloro-5,11-dihydro-5,11-dimethyl-6H-dipyrido[3,2-b:2',3'-e][1,4]diazepin-6-one and (t-butoxycarbonyl)pyrrole in a manner analogous to that described in Example 23.
Quellen und Nachweise
- ORD-Eintrag
- ord-384e0007a95c4be98b9866aa3360abf7
- Quelldatensatz