4-Mercaptophenol → 4-[(4-Hydroxyphenyl)disulfanyl]phenol

HRID 356842

Reaktionsgleichung

Reaktionsgleichung von HRID 356842
[OH:1][C:2]1[CH:7]=[CH:6][C:5]([SH:8])=[CH:4][CH:3]=1>CS(C)=O>[OH:1][C:2]1[CH:7]=[CH:6][C:5]([S:8][S:8][C:5]2[CH:6]=[CH:7][C:2]([OH:1])=[CH:3][CH:4]=2)=[CH:4][CH:3]=1

Komponenten

3

Edukt 1

HCID 2401474-Mercaptophenol

Produkt 1

HCID 2806654-[(4-Hydroxyphenyl)disulfanyl]phenol

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 679Dimethyl SulfoxideLösungsmittel

Versuchsvorschrift

p-Hydroxybenzenethiol (25 g) was dissolved in DMSO (155 ml) and the solution was stirred for 4 hours and poured into ice water (1 L). The precipitated crystals were dried under reduced pressure to give bis(p-hydroxyphenyl)disulfide quantitatively.

Aufarbeitung

  1. customThe precipitated crystals were dried under reduced pressure

Quellen und Nachweise

ORD-Eintrag
ord-7085146c16bc4d318e7e2210028e4e8b
Quelldatensatz
uspto-grants-1998_11
Patentnummer
US05840716

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