Dimethylamine → 2-[1-(Ethoxyimino)propyl]-3-hydroxy-5-(2,6-dimethyl-3-dimethylsulfamoylphenyl)cyclohex-2-en-1-one

HRID 35768

Reaktionsgleichung

Reaktionsgleichung von HRID 35768
[OH:1][C:2]1[CH2:7][CH:6]([C:8]2[C:13]([CH3:14])=[CH:12][CH:11]=[CH:10][C:9]=2[CH3:15])[CH2:5][C:4](=[O:16])[C:3]=1[C:17](=O)[CH2:18][CH3:19].Cl[S:22]([OH:25])(=O)=[O:23].[CH3:26][NH:27][CH3:28].Cl.[CH2:30]([O:32][NH2:33])[CH3:31]>>[CH2:30]([O:32][N:33]=[C:17]([C:3]1[C:4](=[O:16])[CH2:5][CH:6]([C:8]2[C:13]([CH3:14])=[CH:12][CH:11]=[C:10]([S:22](=[O:25])(=[O:23])[N:27]([CH3:28])[CH3:26])[C:9]=2[CH3:15])[CH2:7][C:2]=1[OH:1])[CH2:18][CH3:19])[CH3:31]

Komponenten

5

Edukt 4

HCID 674DimethylamineHCID 24638Chlorosulfonic acidHCID 76850O-ethylhydroxylamine hydrochlorideHCID 178458832HCID 178458832, Verbindung

Produkt 1

HCID 1359739802-[1-(Ethoxyimino)propyl]-3-hydroxy-5-(2,6-dimethyl-3-dimethylsulfamoylphenyl)cyclohex-2-en-1-one

Versuchsvorschrift

2-[1-(Ethoxyimino)propyl]-3-hydroxy-5-(2,6-dimethyl-3-dimethylsulfamoylphenyl)cyclohex-2-en-1-one (5) was prepared from 3-hydroxy-5-(2,6-dimethylphenyl)-2-propionylcyclohex-2-en-1-one, chlorosulfonic acid, dimethylamine, and ethoxyamine hydrochloride following essentially the same procedure as that described in Example 5.

Quellen und Nachweise

ORD-Eintrag
ord-5cb6474f52844c2bba022377de34628a
Quelldatensatz
uspto-grants-1988_08
Patentnummer
US04767879

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