HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
tert-Butyl isocyanate → 1-Phenyl-3-t-butyl hydantoin
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | tert-Butyl isocyanate | HCID 62412 | — |
| Edukt | N-Phenylglycine | HCID 66025 | — |
| Lösungsmittel | Toluene | HCID 1140 | — |
| Produkt | 1-Phenyl-3-t-butyl hydantoin | HCID 12263354 | 60% |
Reaktionsschritte
A mixture of N-phenyl glycine (0.1 mole), t-butyl isocyanate (0.12 mole) and toluene (30 ml) was refluxed for 5 hours and then cooled. The product was collected by filtration and crystallized from ethanol to produce 0.06 mole of the aforedescribed product having a melting point of 116° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04464387 |
| Quelldatensatz | uspto-grants-1984_08 |
| ORD ID | ord-0dbebeb7dd46429c87e48675660834df |
| Quellennotiz | uspto-grants-1984_08 |