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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 358258Erstellt: 24. Oktober 2026

Methanimidic acid, N-phenyl-, ethyl ester → HCID 178482101, Verbindung

https://huagongshe.com/de/reaction/358258

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktMethanimidic acid, N-phenyl-, ethyl esterHCID 111236—
EduktHCID 178507418HCID 178507418—
LösungsmittelAcetoneHCID 180—
ProduktHCID 178482101HCID 17848210156,9%

Reaktionsschritte

Five grams of 4-(4-aminophenyl)-1-H-imidazole were added to a solution of 4.6 gm of ethyl N-phenyl-formimidate [Org. Synth., 35, 65 (1965)] in 25 ml of acetone. After stirring for four hours at room temperature, the solid that separated was filtered and dried under vacuum. The product was treated with acetone and acidified with glacial acetic acid. N-Phenyl-N'-[4-(imidazol-4-yl]-formamidine crystallized as acetate salt which was filtered to give 4.6 gm of the desired product.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04465841
Quelldatensatzuspto-grants-1984_08
ORD IDord-699e0aeb59e647b5813b7ec3e468f229
Quellennotizuspto-grants-1984_08