HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3-Methyl-2-buten-1-OL → Ethyl 3,3-dimethylpent-4-enoate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3-Methyl-2-buten-1-OL | HCID 11173 | — |
| Edukt | Ethyl ortho-acetate | HCID 86598186 | — |
| Katalysator | Phosphoric Acid | HCID 1004 | — |
| Produkt | Ethyl 3,3-dimethylpent-4-enoate | HCID 82262 | 79% |
Reaktionsschritte
A mixture of 4.3 g of 3-methyl-2-buten-1-ol, 16.2 g of ethyl orthoacetate and 3 drops of phosphoric acid was reacted as described in Example V A to give 6.15 g (79% yield) of ethyl 3,3-dimethyl-4-pentenoate, b.p. 87°-88°/58 mm.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04999451 |
| Quelldatensatz | uspto-grants-1991_03 |
| ORD ID | ord-3e7cb3b1ca404cda836c93bd7abb5b97 |
| Quellennotiz | uspto-grants-1991_03 |