Benzoyl chloride → HCID 18963390, Verbindung

Reaktionsgleichung

[C:1]([C:4]1[CH2:9][CH2:8][CH2:7][NH:6][CH:5]=1)(=[O:3])[CH3:2].[C:10](Cl)(=[O:17])[C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1.CC(N1CCCC(C(C)=O)=C1)C>>[C:10]([N:6]1[CH2:7][CH2:8][CH2:9][C:4]([C:1]([CH3:2])=[O:3])=[CH:5]1)(=[O:17])[C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1

Komponenten

Edukt 3

HCID 7412Benzoyl chloride

HCID 32845951-(1,4,5,6-Tetrahydropyridin-3-yl)ethanone

HCID 18963350HCID 18963350, Verbindung

Produkt 1

HCID 18963390HCID 18963390, Verbindung

Versuchsvorschrift

Methyl 1-benzoyl-1,4,5,6-tetrahydro-3-pyridyl ketone was prepared from 3-acetyl-1,4,5,6-tetrahydropyridine and benzoyl chloride according to the procedure of Part (b) of Example 1. The product was recrystallised from ethanol/water m.pt. 93-95°C.