Benzoyl chloride → HCID 20064883, Verbindung
Reaktionsgleichung
[CH3:1][C:2]1([CH3:13])[CH2:11][C:10]2[NH:9][CH2:8][CH2:7][CH2:6][C:5]=2[C:4](=[O:12])[CH2:3]1.[C:14](Cl)(=[O:21])[C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1.CC(N1CCCC(C(C)=O)=C1)C>>[CH3:1][C:2]1([CH3:13])[CH2:11][C:10]2[N:9]([C:14](=[O:21])[C:15]3[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=3)[CH2:8][CH2:7][CH2:6][C:5]=2[C:4](=[O:12])[CH2:3]1Komponenten
4
Versuchsvorschrift
7,7 Dimethyl-1,2,3,4,7,8-hexahydro-quinolin5(6H)-one was reacted with benzoyl chloride according to the procedure of Part (b) of Example 1 to give 7,7-dimethyl-1,2,3,4,7,8-hexahydro-1-benzoyl-quinolin-5(6H)-one (19) as a yellow solid.
Quellen und Nachweise
- ORD-Eintrag
- ord-b1c1861f5bb14451838ca6be14ef30a2