HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Sodium hydride → 3-Cyano-2-(6-dimethylaminohexyloxy)pyridine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Sodium hydride | HCID 24758 | — |
| Edukt | 6-Dimethylaminohexan-1-ol | HCID 74623 | — |
| Edukt | 2-Chloronicotinonitrile | HCID 81079 | — |
| Edukt | Sodium | HCID 5360545 | — |
| Lösungsmittel | Toluene | HCID 1140 | — |
| Produkt | 3-Cyano-2-(6-dimethylaminohexyloxy)pyridine | HCID 15135639 | — |
Reaktionsschritte
6-Dimethylaminohexanol is converted into its sodium salt with sodium hydride in toluene, followed by reaction of the sodium salt with 2-chloro-3-cyanopyridine to give 3-cyano-2-(6-dimethylaminohexyloxy)pyridine.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05001137 |
| Quelldatensatz | uspto-grants-1991_03 |
| ORD ID | ord-92f31da8126842d3985a154613783827 |
| Quellennotiz | uspto-grants-1991_03 |