HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
O-Xylene → HCID 18788042, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | O-Xylene | HCID 7237 | — |
| Edukt | N-butyl-N-(2-methylprop-2-eneyl)aniline | HCID 54010992 | — |
| Katalysator | Zincchloride | HCID 3007855 | — |
| Produkt | HCID 18788042 | HCID 18788042 | — |
Reaktionsschritte
A mixture of N-butyl-N-(2-methylprop-2-eneyl)aniline (9.6 parts), zinc chloride (6.12 parts) and xylene (20 parts) was heated under reflux with vigorous stirring for 4.75 hours. The cooled mixture was filtered and the organic phase evaporated to leave 1-butyl-2,2-dimethylindoline (5.3 parts).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05865857 |
| Quelldatensatz | uspto-grants-1999_02 |
| ORD ID | ord-c307e14b853947698fc2fcb3cdb64320 |
| Quellennotiz | uspto-grants-1999_02 |