HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Ferulic Acid → Dihydroferulic Acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Ferulic Acid | HCID 445858 | — |
| Katalysator | HCID 178418390 | HCID 178418390 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Produkt | Dihydroferulic Acid | HCID 14340 | 95,5% |
Reaktionsschritte
20.0 g of Ferulic acid was dissolved in 250 ml of methanol and subjected to catalytic reduction under normal pressure for 3 hours in the presence of 10% palladium carbon catalyst (50% wet type). After removing the catalyst by filtration, the resulting filtrate was concentrated to collect precipitated crystals by filtration, thereby obtaining 19.3 g of 3-(4-hydroxy-3-methoxy-phenyl)propionic acid.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05866577 |
| Quelldatensatz | uspto-grants-1999_02 |
| ORD ID | ord-2b9785a46e3447c889ec800be50ab02b |
| Quellennotiz | uspto-grants-1999_02 |