(E)-2-(4,6-difluoro-1-indanylidene)acetic acid → (E)-2-(4-fluoro-1-indanylidene)acetyl Chloride

HRID 362833Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 362833
[F:1][C:2]1[CH:10]=[C:9](F)[CH:8]=[C:7]2[C:3]=1[CH2:4][CH2:5]/[C:6]/2=[CH:12]\[C:13]([Cl:15])=[O:14].FC1C=C(F)C=C2C=1CC/C/2=C\C(O)=O>>[F:1][C:2]1[CH:10]=[CH:9][CH:8]=[C:7]2[C:3]=1[CH2:4][CH2:5]/[C:6]/2=[CH:12]\[C:13]([Cl:15])=[O:14]

Komponenten

3

Edukt 2

HCID 10976722(E)-2-(4,6-difluoro-1-indanylidene)acetic acidHCID 10977254(E)-2-(4,6-difluoro-1-indanylidene)acetyl Chloride

Produkt 1

HCID 23293683(E)-2-(4-fluoro-1-indanylidene)acetyl Chloride

Versuchsvorschrift

This compound was prepared in a similar manner to (E)-2-(4,6difluoro-1-indanylidene)acetyl chloride in Example 5f by substituting (E)-2-(4-fluoro-1-indanylidene)acetic acid (5.77 g, 0.03 mol) for (E)-2-(4,6-difluoro-1-indanylidene)acetic acid. The resulting solution was concentrated in vacuo, and the residue was used without further purification.

Aufarbeitung

  1. concentrationThe resulting solution was concentrated in vacuo
  2. customthe residue was used without further purification

Quellen und Nachweise

ORD-Eintrag
ord-04a18eb498ce4517b85679760aa991e6
Quelldatensatz
uspto-grants-1999_02
Patentnummer
US05872118

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