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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 36313Erstellt: 23. Oktober 2026

Anthranilic Acid → N-n-octylanthranilic acid

https://huagongshe.com/de/reaction/36313

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktAnthranilic AcidHCID 227—
EduktSodium HydroxideHCID 14798—
Eduktn-Octyl p-ToluenesulfonateHCID 599296—
LösungsmittelTolueneHCID 1140—
ProduktN-n-octylanthranilic acidHCID 1509028943,1%

Reaktionsbedingungen

Temperatur120 °C

Reaktionsschritte

To a solution of anthranilic acid in toluene, n-octyl p-toluenesulfonate prepared according to the conventional method was added and the mixture was refluxed at 120° C. After 6 hours, an aqueous solution of sodium hydroxide was added and the toluene layer was concentrated. N-n-octylanthranilic acid was obtained from the remaining reactant after the purification by column chromatography with the yield of 43.1%.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05413794
Quelldatensatzuspto-grants-1995_05
ORD IDord-83f0afa4f03c4cc1a583fc651ef4429b
Quellennotizuspto-grants-1995_05