HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Water → 6-Phenylnicotinic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Water | HCID 962 | — |
| Edukt | 5-Methyl-2-phenylpyridine | HCID 47467 | — |
| Edukt | Potassium Permanganate | HCID 516875 | — |
| Produkt | 6-Phenylnicotinic acid | HCID 120118 | — |
Reaktionsschritte
A suspension of 2-phenyl-5-methyl pyridine (1.03 g, 6.09 mmol) and potassium permanganate (2.89 g, 18.3 mmol), in water (25 mL) was heated at reflux for 2 hours. The reaction was allowed to cool to ambient temperature and filtered through celite to remove the solids. Acetic acid (1 mL) was added to the colourless filtrate and the product was collected as a white solid by filtration.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05872136 |
| Quelldatensatz | uspto-grants-1999_02 |
| ORD ID | ord-6e644e5ebedd4852bf22e76bd7adb84c |
| Quellennotiz | uspto-grants-1999_02 |