HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 36320Erstellt: 23. Oktober 2026
N-Methylbutylamine → N-butyl-N-methylacetamide dimethyl acetal
https://huagongshe.com/de/reaction/36320
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | N-Methylbutylamine | HCID 8068 | — |
| Edukt | 1,1-Dimethoxyethyl(dimethyl)amine | HCID 87835 | — |
| Produkt | N-butyl-N-methylacetamide dimethyl acetal | HCID 19379602 | — |
Reaktionsschritte
6.1 g (0.07 mol) of n-butylmethylamine are stirred with 9.3 g (0.07 mol) of N,N-dimethylacetamide dimethyl acetal for 24 hours under reflux at a bath temperature of 130° C. Subsequent vacuum distillation gives N-butyl-N-methylacetamide dimethyl acetal, bp 72°-75° C./31 mbar.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patentnummer | US05413994 |
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| Quelldatensatz | uspto-grants-1995_05 |
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| ORD ID | ord-958d91a3e3b94844878d9825f3955bb5 |
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| Quellennotiz | uspto-grants-1995_05 |
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