Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Phenol | HCID 996 | — |
| Edukt | Potassium Hydroxide | HCID 14797 | — |
| Edukt | 2,2'-Bis(bromomethyl)-1,1'-biphenyl | HCID 251962 | — |
| Katalysator | Benzyl triethylammonium chloride | HCID 66133 | — |
| Lösungsmittel | Dichloromethane | HCID 6344 | — |
| Produkt | 2,2'-Bis(phenoxymethyl)biphenyl | HCID 53737607 | — |
Reaktionsschritte
A mixture of 25.0 g (73.5 mmol) of 2,2'-bis(bromomethyl)biphenyl, 14.2 g (151 mmol) of phenol, 14.7 g (261 mmol) of pulverized potassium hydroxide and 3.41 g (15 mmol) of triethylbenzylammonium chloride is admixed with 120 ml of dichloromethane and stirred for 5 hours at 40° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patentnummer | US05874642 |
|---|
| Quelldatensatz | uspto-grants-1999_02 |
|---|
| ORD ID | ord-9668b42c33fa4570bcfe893d5ace0f55 |
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| Quellennotiz | uspto-grants-1999_02 |
|---|
