HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
N-(2-Acetylphenyl)acetamide → HCID 54331422, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | N-(2-Acetylphenyl)acetamide | HCID 21306 | — |
| Edukt | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| Lösungsmittel | Toluene | HCID 1140 | — |
| Produkt | HCID 54331422 | HCID 54331422 | 63,6% |
Reaktionsschritte
A suspension of 48 g of N-[2-(1-oxo-1-ethanyl)phenyl]acetamide and 38 g of N,N-dimethylformamide dimethyl acetal in 150 ml of toluene was heated at reflux for about 16 hours, then concentrated in vacuo to a solid. The solid was recrystallized from 1-chlorobutane to yield 40 g of the title compound; m.p. 90°-95° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04606755 |
| Quelldatensatz | uspto-grants-1986_08 |
| ORD ID | ord-93ec883c9ccb4b28914aad0f2c2c7668 |
| Quellennotiz | uspto-grants-1986_08 |