HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Thionyl Chloride → Benzoyl chloride, 4-(hexyloxy)-
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Thionyl Chloride | HCID 24386 | — |
| Edukt | 4-(Hexyloxy)benzoic acid | HCID 70834 | — |
| Produkt | Benzoyl chloride, 4-(hexyloxy)- | HCID 170235 | 98% |
Reaktionsschritte
Thionyl chloride (485 g of 98%, 4.00 mol) was added dropwise to 300 g (1.35 mol) of 4-hexyloxybenzoic acid. The resulting mixture was refluxed under nitrogen for 2 hours. Distillation yielded 318 g (98%) of 4-hexyloxybenzoyl chloride [boiling point 149°-153° C. (7.5 mm)].
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04606838 |
| Quelldatensatz | uspto-grants-1986_08 |
| ORD ID | ord-37bb1f97559e446dbcf78a51799a51db |
| Quellennotiz | uspto-grants-1986_08 |