2-Undecanone → Ethyl 2-(2-Butyl)-3-hydroxy-3-methyldodecanoate

HRID 365015

Reaktionsgleichung

[CH3:1][C:2](=[O:12])[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH3:11].[CH3:13][CH:14]([CH2:21][CH3:22])[CH2:15][C:16]([O:18][CH2:19][CH3:20])=[O:17]>>[CH3:13][CH:14]([CH:15]([C:2]([OH:12])([CH3:1])[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH3:11])[C:16]([O:18][CH2:19][CH3:20])=[O:17])[CH2:21][CH3:22]

Komponenten

Edukt 2

HCID 81632-Undecanone

HCID 560255Ethyl 3-methylpentanoate

Produkt 1

HCID 13742290Ethyl 2-(2-Butyl)-3-hydroxy-3-methyldodecanoate

Versuchsvorschrift

Pyrolysis of a sample of the prepared hydroxy-ester at about 300° C. for 2 minutes yields a 1:1 mixture of 2-undecanone and ethyl 3-methylvalerate.

Quellen und Nachweise

ORD-Eintrag: ord-b0811ba8b5114215947a50cb777aabb6
Quelldatensatz: uspto-grants-1986_08
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US04607118

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