Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Hydrogen Peroxide | HCID 784 | — |
| Edukt | Ethylenediaminetetraacetic Acid | HCID 6049 | — |
| Edukt | Butyl imino dipropionic acid | HCID 131718997 | — |
| Lösungsmittel | Water | HCID 962 | — |
| Produkt | HCID 178444799 | HCID 178444799 | — |
Reaktionsschritte
100 g butyl imino dipropionic acid (0.46 mol) from example 7a was dissolved in 100 g H2O, whereupon 0.10 g EDTA was added and the temperature was increased to 50° C. After 30 minutes 3.2 g (0.475 mol) 50% hydrogen peroxide was added by drops during 20 minutes and the mixture reacted for 2 hours at 75° C. under a reflux cooler. Then the water was evaporated at 40° C. until a slightly yellow-brown oil formed.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patentnummer | US05415668 |
|---|
| Quelldatensatz | uspto-grants-1995_05 |
|---|
| ORD ID | ord-21e0230d66d34335bfad3ff73829e671 |
|---|
| Quellennotiz | uspto-grants-1995_05 |
|---|
