HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Propenoic acid, 3-(4-chlorophenyl)- → 3-(4-Chlorophenyl)prop-2-enoyl chloride
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Propenoic acid, 3-(4-chlorophenyl)- | HCID 15371 | — |
| Edukt | Thionyl Chloride | HCID 24386 | — |
| Lösungsmittel | Benzene | HCID 241 | — |
| Produkt | 3-(4-Chlorophenyl)prop-2-enoyl chloride | HCID 53411294 | — |
Reaktionsschritte
100 ml of benzene was added to 18.3 grams of p-chlorocinnamic acid. 12 ml of thionyl chloride was added dropwise slowly thereto at ambient temperature. The temperature was elevated to 80° C. and the heating was continued until foaming ceased. Benzene and thionyl chloride were distilled off and the residue was dried thoroughly under reduced pressure.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05415780 |
| Quelldatensatz | uspto-grants-1995_05 |
| ORD ID | ord-92d1af992d9442b597102890f8b434d9 |
| Quellennotiz | uspto-grants-1995_05 |