HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Bromoacetyl chloride → 4-Bromoacetyl-2,3,4,5-tetrahydro-1,4-benzothiazepine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Bromoacetyl chloride | HCID 89602 | — |
| Edukt | 2,3,4,5-Tetrahydrobenzo[f][1,4]thiazepine | HCID 12269106 | — |
| Lösungsmittel | Triethylamine | HCID 8471 | — |
| Produkt | 4-Bromoacetyl-2,3,4,5-tetrahydro-1,4-benzothiazepine | HCID 15291657 | 42,1% |
Reaktionsschritte
2,3,4,5-Tetrahydro-1,4-benzothiazepine (4.8 g), triethylamine (5.9 g) and bromoacetyl chloride (5.5 g) were reacted in the same manner as in Experimental Example 1 to give 4-bromoacetyl-2,3,4,5-tetrahydro-1,4-benzothiazepine (3.5 g).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05416066 |
| Quelldatensatz | uspto-grants-1995_05 |
| ORD ID | ord-b064d53212ac4e57835ad8c2d0a85198 |
| Quellennotiz | uspto-grants-1995_05 |