HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1,3,5-Trichlorobenzene → 1,3,5-Trifluorobenzene
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1,3,5-Trichlorobenzene | HCID 7950 | — |
| Edukt | Fluoride Ion | HCID 28179 | — |
| Edukt | 3,5-Difluoroaniline | HCID 96595 | — |
| Produkt | 1,3,5-Trifluorobenzene | HCID 9745 | — |
Reaktionsschritte
In a further embodiment, the present invention relates to a method for the two step preparation of 3,5-difluoroaniline from 1,3,5-trichlorobenzene. First, an amount of 1,3,5-trichlorobenzene is reacted with a fluoride-containing compound to obtain 1,3,5-trifluorobenzene. Second, the 1,3,5-trifluorobenzene is reacted with aqueous ammonia and a metal oxide or metal hydroxide to obtain the product 3,5-difluoroaniline.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06127577 |
| Quelldatensatz | uspto-grants-2000_10 |
| ORD ID | ord-45e0cbdb38d34daab543f555c607bb71 |
| Quellennotiz | uspto-grants-2000_10 |