HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Chlorotrimethylsilane → 2-Chloro-n-ethyl-6-(trimethylsilyl)benzamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Chlorotrimethylsilane | HCID 6397 | — |
| Edukt | 2-chloro-N-ethylbenzamide | HCID 347962 | — |
| Produkt | 2-Chloro-n-ethyl-6-(trimethylsilyl)benzamide | HCID 18630379 | — |
Reaktionsschritte
The compound of Example f (2.2 g, 0.012 mol) was reacted with TMSCl (3.91 g, 0.036 mol) using General Method A. The title compound was recrystallized from ether/hexanes as a solid. m.p. 105-107° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06133252 |
| Quelldatensatz | uspto-grants-2000_10 |
| ORD ID | ord-26982034b01c4721a756e22a17cbba3f |
| Quellennotiz | uspto-grants-2000_10 |