HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Chlorotriethylsilane → HCID 18630182, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Chlorotriethylsilane | HCID 13819 | — |
| Edukt | 2-Chloro-N,N-diethylbenzamide | HCID 82566 | — |
| Produkt | HCID 18630182 | HCID 18630182 | — |
Reaktionsschritte
The title compound was prepared according to General Method A from the compound of Example e and 1.4 eq chlorotriethylsilane. Purification by HPLC with 1:19 ethyl acetate/hexanes gave 6.0 g of the desired product as a clear oil, a 92% yield.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06133252 |
| Quelldatensatz | uspto-grants-2000_10 |
| ORD ID | ord-964a76a7c96a4af4b5016d01d8c6ca28 |
| Quellennotiz | uspto-grants-2000_10 |