HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Chlorodimethylphenylsilane → n,n-Diethyl-2-chloro-6-(dimethylphenylsilyl)benzamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Chlorodimethylphenylsilane | HCID 13029 | — |
| Edukt | 2-Chloro-N,N-diethylbenzamide | HCID 82566 | — |
| Produkt | n,n-Diethyl-2-chloro-6-(dimethylphenylsilyl)benzamide | HCID 54348567 | — |
Reaktionsschritte
The title compound was prepared from the compound of Example e and 1.1 eq dimethylphenylsilyl chloride according to General Method A. Purification by HPLC with 1:9 ethyl acetate/hexanes gave 6.3 g of the desired product as a clear oil, a 91% yield.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06133252 |
| Quelldatensatz | uspto-grants-2000_10 |
| ORD ID | ord-2369a7a7151e4673a5f780d38ab28100 |
| Quellennotiz | uspto-grants-2000_10 |