HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Silane, chloro(chloromethyl)dimethyl- → n-Ethyl-2-chloro-6-[(chloromethyl)dimethylsilyl]benzamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Silane, chloro(chloromethyl)dimethyl- | HCID 74393 | — |
| Edukt | 2-chloro-N-ethylbenzamide | HCID 347962 | — |
| Produkt | n-Ethyl-2-chloro-6-[(chloromethyl)dimethylsilyl]benzamide | HCID 18630074 | — |
Reaktionsschritte
The title compound was prepared from the compound of Example f and 2.0 eq (chloromethyl)dimethylsilyl chloride according to General Method C. Recrystallization from ethyl acetate gave 3.0 g of the desired compound as a white solid, a 52% yield. m.p. 88-89° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06133252 |
| Quelldatensatz | uspto-grants-2000_10 |
| ORD ID | ord-5559485b8ba34a3ba66d94109c8a8114 |
| Quellennotiz | uspto-grants-2000_10 |