HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-chloro-N-ethylbenzamide → n-Ethyl-2-chloro-6-(ethenyldimethylsilyl)benzamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-chloro-N-ethylbenzamide | HCID 347962 | — |
| Edukt | Chloro(dimethyl)vinylsilane | HCID 519368 | — |
| Produkt | n-Ethyl-2-chloro-6-(ethenyldimethylsilyl)benzamide | HCID 18630374 | — |
Reaktionsschritte
The title compound was prepared from the compound of Example f and 1.5 eq vinyldimethylsilyl chloride according to General Method C. Purification by HPLC with 1:4 ethyl acetate/hexanes gave 630 mg of the desired product as a white solid, a 9% yield. m.p. 86-89° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06133252 |
| Quelldatensatz | uspto-grants-2000_10 |
| ORD ID | ord-e516eaac738c431c89d10dde00a955ba |
| Quellennotiz | uspto-grants-2000_10 |