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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 369538Erstellt: 24. Oktober 2026

p-n-Octadecyloxybenzoic acid → 4-(trans-3-Decenyloxy)-benzoic acid

https://huagongshe.com/de/reaction/369538

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Eduktp-n-Octadecyloxybenzoic acidHCID 139993—
EduktLithium hydroxide, monohydrateHCID 168937—
EduktMethyl-4-(trans-3-decenyloxy)-benzoateHCID 18521096—
LösungsmittelMethanolHCID 887—
Produkt4-(trans-3-Decenyloxy)-benzoic acidHCID 18521103—

Reaktionsschritte

Ester 35h (600 mg, 2.07 mmol), and lithium hydroxide monohydrate (867 mg, 20.7 mmol) in 20 ml methanol were reacted according to the procedure for compound 36a. The yield was 500 mg (87%) of a white powder which was not quite pure (95%). The product was used without further purification.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS06139771
Quelldatensatzuspto-grants-2000_10
ORD IDord-b213ca41cefd427f9bb23e37e0e5988d
Quellennotizuspto-grants-2000_10