HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Methyl bromoacetate → N-methoxycarbonylmethyl-N-[2-nitro-5-(2-chloro-4-trifluoromethylphenoxy)phenyl]ethoxyamine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Methyl bromoacetate | HCID 60984 | — |
| Edukt | O-ethylhydroxylamine hydrochloride | HCID 76850 | — |
| Edukt | Benzene, 2-chloro-1-(3,4-dinitrophenoxy)-4-(trifluoromethyl)- | HCID 156238 | — |
| Edukt | O-phenethylhydroxylamine | HCID 202940 | — |
| Edukt | N-[2-nitro-5-(2-chloro-4-trifluoromethylphenoxy)phenyl]ethoxyamine | HCID 70487366 | — |
| Produkt | N-methoxycarbonylmethyl-N-[2-nitro-5-(2-chloro-4-trifluoromethylphenoxy)phenyl]ethoxyamine | HCID 86740181 | — |
Reaktionsschritte
Following the procedure of Example 29, N-[2-nitro-5-(2-chloro-4-trifluoromethylphenoxy)phenyl]ethoxyamine is prepared from 4-(2-chloro-4-trifluoromethylphenoxy)1,2-dinitrobenzene and ethoxyamine hydrochloride. The resulting N-phenylethoxyamine is then reacted with methyl bromoacetate, following the methods of this example, to yield N-methoxycarbonylmethyl-N-[2-nitro-5-(2-chloro-4-trifluoromethylphenoxy)phenyl]ethoxyamine.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04526608 |
| Quelldatensatz | uspto-grants-1985_07 |
| ORD ID | ord-c15788ec88a2485daccd358bdb82bb9a |
| Quellennotiz | uspto-grants-1985_07 |