HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Indole-3-Acetic Acid → HCID 12219383, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Indole-3-Acetic Acid | HCID 802 | — |
| Edukt | Oxalyl chloride | HCID 65578 | — |
| Lösungsmittel | Dimethylformamide | HCID 6228 | — |
| Lösungsmittel | Dichloromethane | HCID 6344 | — |
| Produkt | HCID 12219383 | HCID 12219383 | — |
Reaktionsschritte
To indole-3-acetic acid (186 mg, 1.06 mmol) in 3.5 mL of methylene chloride and 0.009 mL of dimethylformamide, oxalyl chloride (2 M in methylene chloride, 0.64 mL, 1.27 mmol) was added. The mixture was stirred at room temperature for 1 hour and concentrated to give 1H-indole-3-acetyl chloride.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05420123 |
| Quelldatensatz | uspto-grants-1995_05 |
| ORD ID | ord-b5bb6f04c7054cc0b42ddca249e133b1 |
| Quellennotiz | uspto-grants-1995_05 |