HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
N-Methylbenzamide → N-Methylbenzimidoyl chloride
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | N-Methylbenzamide | HCID 11954 | — |
| Edukt | Thionyl Chloride | HCID 24386 | — |
| Produkt | N-Methylbenzimidoyl chloride | HCID 576277 | 91% |
Reaktionsschritte
N-Methyl benzamide (55.97 g., 418 mmole) and thionyl chloride (114.7 g, 0.96 mole) were treated as in Example I. Yield 58.4 g (91%) of the title compound, b.p. 80°-90° C. (~0.1 mm Hg).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04528382 |
| Quelldatensatz | uspto-grants-1985_07 |
| ORD ID | ord-a8c72cef2c564185b95a22d00e3d16a7 |
| Quellennotiz | uspto-grants-1985_07 |