Hydrochloric Acid → Dodecylammonium chloride

HRID 371254Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 371254
[CH2:1]([NH2:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12].[ClH:14]>C(Cl)Cl>[ClH:14].[CH2:1]([NH2:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12]

Komponenten

4

Edukt 2

HCID 313Hydrochloric AcidHCID 13583Dodecylamine

Produkt 1

HCID 458426Dodecylammonium chlorideAusbeute 95,5 %

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 6344DichloromethaneLösungsmittel

Reaktionsbedingungen

Temperatur
0 °C

Versuchsvorschrift

Dodecylamine (85 g, 0.46 mol) was dissolved in methylene chloride (500 mL). The solution was cooled to 0° C., and saturated with anhydrous hydrogen chloride (45 minutes). The white, crystalline solid was separated and dried in vacuum over phosphorus pentoxide, to provide 97.5 g (95.5%) of n-dodecylamine hydrochloride.

Aufarbeitung

  1. customThe white, crystalline solid was separated
  2. dry with materialdried in vacuum over phosphorus pentoxide

Quellen und Nachweise

ORD-Eintrag
ord-3610f441decb46118ba667e34d25705d
Quelldatensatz
uspto-grants-1985_07
Patentnummer
US04530714

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