Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Acetic Acid | HCID 176 | — |
| Edukt | Ethyl 4,4,4-trifluoroacetoacetate | HCID 67793 | — |
| Edukt | HCID 178509258 | HCID 178509258 | — |
| Lösungsmittel | Diethyl Ether | HCID 3283 | — |
| Produkt | HCID 178516129 | HCID 178516129 | — |
Reaktionsschritte
In an 8 ml acetic acid solution of 1.07 g of 3-amino-4-(4phenylthiophenyl)pyrazole, 0.6 ml of ethyl 4,4,4-trifluoroacetoacetate was added and stirred for 2 hours at 100° C. After allowing to cool, ether was added, and the precipitate was filtered and dried, and the title compound was obtained (200 mg, 13%).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patentnummer | US05420128 |
|---|
| Quelldatensatz | uspto-grants-1995_05 |
|---|
| ORD ID | ord-7764346d11f4457dbeff3dc3fdad1d99 |
|---|
| Quellennotiz | uspto-grants-1995_05 |
|---|
