3,4-Dimethylaniline → 2,2'-Dithiobis[N-(3,4-dimethylphenyl)benzamide]

Beteiligte Stoffe

Reaktionsschritte

This compound was prepared according to the general method of Example 77 using 2,2'-dithiobisbenzoyl chloride (1.12 g, 3.26 mmol) in 25 mL of dichloromethane and 3,4-dimethylaniline (0.79 g, 6.52 mmol) in 8 mL of pyridine. The crude product was triturated with ethyl ether and filtered to yield 0.28 g of the title compound, mp 224°-227° C.

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