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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 371753Erstellt: 25. Oktober 2026

6-Methoxyquinoline → Quinoline, 1,2,3,4-tetrahydro-6-methoxy-

https://huagongshe.com/reaction/371753

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
Edukt6-MethoxyquinolineHCID 14860—
KatalysatorPalladiumHCID 23938—
LösungsmittelEthanolHCID 702—
ProduktQuinoline, 1,2,3,4-tetrahydro-6-methoxy-HCID 6711394,6%

Reaktionsschritte

6-Methoxyquinoline (1.00g) was dissolved in absolute ethanol (20 ml) and hydrogenated under pressure in the presence of 10% palladium on charcoal (0.10g) with shaking for about 40 hours. Filtration and evaporation to dryness of the filtrate gave 1,2,3,4-tetrahydro-6-methoxyquinoline as a light-brown gum (0.97g). The structure was supported by nmr spectrum.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04087561
Quelldatensatzuspto-grants-1978_05
ORD IDord-1d27416b936e4f4b9c7fc294a512a2d7
Quellennotizuspto-grants-1978_05