Hydrochloric Acid → 2-[4-(2-Methoxyphenyl)piperazin-1-yl]ethanamine trihydrochloride

HRID 37192Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 37192
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[N:9]1[CH2:14][CH2:13][N:12]([CH2:15][CH2:16][NH:17]C(C2C=CC=CC=2)(C2C=CC=CC=2)C2C=CC=CC=2)[CH2:11][CH2:10]1.[ClH:37]>CO>[ClH:37].[ClH:37].[ClH:37].[CH3:1][O:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[N:9]1[CH2:10][CH2:11][N:12]([CH2:15][CH2:16][NH2:17])[CH2:13][CH2:14]1

Komponenten

4

Edukt 2

HCID 313Hydrochloric AcidHCID 157182882-[4-(2-Methoxyphenyl)piperazin-1-yl]-N-(triphenylmethyl)ethanamine

Produkt 1

HCID 199348082-[4-(2-Methoxyphenyl)piperazin-1-yl]ethanamine trihydrochloride

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 887MethanolLösungsmittel

Versuchsvorschrift

9.24 g of 2-[4-(2-methoxyphenyl)piperazin-1-yl)-N-(triphenylmethyl)ethanamine are dissolved in 400 ml of methanol and, after homogenization, a stream of gaseous hydrochloric acid is passed into the solution for 10 min. The precipitate is collected, rinsed with methanol and dried under vacuum. 5.33 g of white solid are obtained.

Aufarbeitung

  1. customThe precipitate is collected
  2. washrinsed with methanol
  3. customdried under vacuum

Quellen und Nachweise

ORD-Eintrag
ord-0f7caca2e5c54b8b9c8794e8848e7290
Quelldatensatz
uspto-grants-1995_05
Patentnummer
US05420130

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