HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-Hexyne → 1-(4-Bromophenyl) 2-heptyn-1-one
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-Hexyne | HCID 12732 | — |
| Edukt | 4-Bromobenzoyl chloride | HCID 68515 | — |
| Lösungsmittel | Triethylamine | HCID 8471 | — |
| Produkt | 1-(4-Bromophenyl) 2-heptyn-1-one | HCID 54449136 | — |
Reaktionsschritte
The following were stirred at ambient temperature for about 2 hours 30 minutes, 49 ml of 1-hexyne, 75 ml of triethylamine, 40 mg of cuprous iodide, 40 mg of bis triphenylphosphine palladium dichloride and 9 g of parabromobenzoyl chloride.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05420138 |
| Quelldatensatz | uspto-grants-1995_05 |
| ORD ID | ord-63ea4cacfe084abf827121e185cfa069 |
| Quellennotiz | uspto-grants-1995_05 |