Hydrogen Bromide → 3-(3-Bromopropyl)pyridine
Reaktionsgleichung
[N:1]1[CH:6]=[CH:5][CH:4]=[C:3]([CH2:7][CH2:8][CH2:9]O)[CH:2]=1.[BrH:11]>>[N:1]1[CH:6]=[CH:5][CH:4]=[C:3]([CH2:7][CH2:8][CH2:9][Br:11])[CH:2]=1Komponenten
3
Versuchsvorschrift
To 17.0 g (124 moles) of 3-(3-pyridyl)-1-propanol was added 240 mL of 48% hydrobromic acid. The mixture was heated under reflux for 4 hours, and then evaporated to dryness to afford the hydrobromide salt of 3-(3-pyridyl)-1-bromopropane as an oil in quantitative yield.
Aufarbeitung
- temperatureThe mixture was heated
- temperatureunder reflux for 4 hours
- customevaporated to dryness
Quellen und Nachweise
- ORD-Eintrag
- ord-d62f1374cf5c45a8a395275ffd52cb2d
- Quelldatensatz
- uspto-grants-1996_01
- Patentnummer
- US05480892
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