2-Amino-3-methylbenzamide → 3-Methyl-2-(2-n-propoxyphenyl)benzamide
Reaktionsgleichung
N[C:2]1[C:10]([CH3:11])=[CH:9][CH:8]=[CH:7][C:3]=1[C:4]([NH2:6])=[O:5].[CH2:12]([O:15][C:16]1[CH:24]=[CH:23][CH:22]=[CH:21][C:17]=1C(Cl)=O)[CH2:13][CH3:14]>>[CH3:11][C:10]1[C:2]([C:17]2[CH:21]=[CH:22][CH:23]=[CH:24][C:16]=2[O:15][CH2:12][CH2:13][CH3:14])=[C:3]([CH:7]=[CH:8][CH:9]=1)[C:4]([NH2:6])=[O:5]Komponenten
3
Versuchsvorschrift
The title compound was prepared from 2-amino-3-methylbenzamide and 2-n-propoxybenzoyl chloride following the procedure of Preparation 5 and was obtained as a colorless solid (71%), m.p. 140°-142° C. Found: C,69.39; H,6.58; N,8.98. C18H20N2O3 requires C,69.21; H,6.45; N,8.97%.
Aufarbeitung
- customthe procedure of Preparation 5
Quellen und Nachweise
- ORD-Eintrag
- ord-c34332d179c54d928a2c3861f8e773f6
- Quelldatensatz
- uspto-grants-1996_01