2-Ethylhexanal → 5-Amino-5-hydroxymethyl-2-(3-heptyl)-1,3-dioxane

Beteiligte Stoffe

Reaktionsschritte

Procedure of Example 2 was repeated with 6.41 g of 2-ethylhexanal and 7.56 g of 2-(hydroxymethyl)-2-nitro-1,3-propanediol to give 11 g of 5-nitro-5-hydroxymethyl-1,3-dioxane derivative, which was reduced and distilled at 175°-178° C. to give 8.7 g of the product.

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